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signi cance in the formation of 3-MCPD. Food Additives and Contaminants, 25, 391 400. Gurr, M.I. (1992). Role of Fats in Food and Nutrition, Elsevier Applied Science, London. Hamlet, C.G., Sadd, P.A., Crews, C., Velisek, J., Baxter, D.E. (2002). Occurrence of 3-chloro-propane-1,2-diol (3-MCPD) and related compounds in foods: a review. Food Additives and Contaminants, 19, 619 631. Brereton, P., Kelly, J., Crews, C., Honour, S., Wood, R., Davies, A. (2001). Determination of 3-chloro-1,2-propanediol in foods and food ingredients by gas chromatography with mass spectrometric detection: collaborative study. Journal of AOAC International, 84, 455 465. British Standards Institution (2004). BS EN. 14573, 2004 Foodstuffs. Determination of 3-monochloropropane-1,2-diol by GC/MS. Nyman, P.J., Diachenko, G.W., Perfetti, G.A. (2003). Determination of 1,3dichloropropanol in soy sauce and related products by using gas chromatography/ mass spectrometry. Food Additives and Contaminants, 20, 903 908. Xu, X., Ren, Y., Wu, P., Han, J., Shen, X. (2006). The simultaneous separation and determination of chloropropanols in soy sauce and other avouring with gas chromatography-mass spectrometry in negative chemical and electron impact ionization modes. Food Additives and Contaminants, 23, 110 119. Chung, W.C., Hui, K.Y., Cheng, S.C. (2002). Sensitive method for the determination of 1,3-dichloropropan-2-ol and 3-chloropropane-1,2-diol in soy sauce by capillary gas chromatography with mass spectrometric detection. Journal of Chromatography, A, 952, 185 192. Abu-El-Haj, S., Bogusz, M.J., Ibrahim, Z., Hassan, H., Al Tufail, M. (2007). Rapid and simple determination of chloropropanols (3-MCPD and 1,3-DCP) in food products using isotope dilution GC MS. Food Control, 18, 81 90. Rodman, L.E., Ross, R.D. (1986). Gas-liquid chromatography of 3-chloropropanediol. Journal of Chromatography, 369, 97 103. Pesselman, R.L., Feit, M.J. (1988). Determination of residual epichlorohydrin and 3-chloropropanediol in water by gas chromatography with electron capture detection. Journal of Chromatography, 439, 448 452. Plantinga, W.J., Van Toorn, W.G., Van Der Stegen, G.H.D. (1991). Determination of 3-chloropropane-1,2-diol in liquid hydrolysed vegetable proteins by capillary gas chromatography with ame ionisation detection. Journal of Chromatography, 555, 311 314. Breitling-Utzmann, C.M., Kobler, H., Herbolzheimer, D., Maier, A. (2003). 3MCPD Occurrence in bread crust and various food groups as well as formation in toast. Deutsche Lebensmittel-Rundschau, 99, 280 285. Divinov , V., Svejkovsk , B., Dole al, M., Vel ek, J. (2004). Determination of free and bound 3-chloropropane-1,2-diol by gas chromatography with mass spectrometric detection using deuterated 3-chloropropane-1,2-diol as internal standard. Czech Journal of Food Sciences, 22, 182 189. Vel ek, J., Dole al, M., Crews, C., Dvor k, T. (2002). Optical isomers of chloropropanediols: mechanisms of their formation and decomposition in protein hydrolysates. Czech Journal of Food Sciences, 20, 161 170.
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58. Kuballa, T., Ruge, W. (2004). Analysis and detection of 3-monochloropropane-1,2diol (3-MCPD) in food by GC/MS/MS. http://www.varianinc.com/cgi-bin/ nav applications/gcms&cid=JLQOILQPFJ (accessed November 2006). 59. Huang, M., Jiang, G., He, B., Liu, J., Zhou, Q., Fu, W., Wu, Y. (2005). Determination of 3-chloropropane-1,2-diol in liquid hydrolyzed vegetable proteins and soy sauce by solid-phase microextraction and gas chromatography/mass spectrometry. Analytical Sciences, 21, 1343 1347. 60. March, J. (1983). Advanced Organic Chemistry: Reactions Mechanisms, and Structure, 2nd edn, McGraw-Hill, Tokyo, pp. 810 811. 61. Dayritt, F.M., Ninonuevo, M.R. (2004). Development of an analytical method for 3-monochloropropane-1,2-diol in soy sauce using 4-heptanone as derivatizing agent. Food Additives and Contaminants, 21, 204 209. 62. Jin, Q., Zhang, Z., Luo, R., Li, J. (2001). Survey of 3-monochloropropane-1,2-diol (3-MCPD) in soy sauce and similar products. Wei Shang Yan Jiu, 30, 60 61. 63. R tho, C., Blanchard, F. (2005). Determination of 3-chloropropane-1,2-diol as its 1,3-dioxolane derivative at the g kg-1 level: application to a wide range of foods. Food Additives and Contaminants, 22, 1189 1197. 64. Wittmann, R. (1991). Determination of dichloropropanols and monochloropropandiols in seasonings and in foodstuffs containing seasonings. Zeitschrift fur Lebensmittel-Untersuchung Und-Forschung, 193, 224 229. 65. Schumacher, R., Nurmi-Legat, J., Oberhauser, A., Kainz, M., Krska, R. (2005). A rapid and sensitive GC-MS method for determination of 1,3-dichloro-2-propanol in water. Analytical and Bioanalytical Chemistry, 382, 366 371. 66. Crews, C., LeBrun, G., Brereton, P.A. (2002). Determination of 1,3-dichloropropanol in soy sauces by automated headspace gas chromatography-mass spectrometry. Food Additives and Contaminants, 19, 343 349. 67. Hasnip, S., Crews, C., Potter, N., Brereton, P. (2005). Determination of 1,3dichloropropanol in soy sauce and related products by headspace gas chromatography with mass spectrometric detection: interlaboratory study. Journal of AOAC International, 88, 1404 1412. 68. Mingxia, Z., Jianke, Z., Junhong, L. (2003). Determination of chloropropanols in expanded foods by gas chromatography. Food and Fermentation Industries, 29, 52 54. 69. Leung, M.K.P., Chiu, B.K.W., Lam, M.H.W. (2003). Molecular sensing of 3-chloro1,2-propanediol by molecular imprinting. Analytica Chimica Acta, 491, 15 25. 70. Xing, X., Cao, Y. (2007). Determination of 3-chloro-1,2-propanediol in soy sauces by capillary electrophoresis with electrochemical detection. Food Control, 18, 167 172. 71. Hamlet, C.G., Sadd, P.A., Gray, D.A. (2004). Chloropropanols and their esters in baked cereal products, in Abstracts of the Division of Agricultural and Food Chemistry 227th Annual Meeting, Anaheim, California, March 28 April 1, 2004 (ed. W. Yokoyama), American Chemical Society, Anaheim. 72. Hamlet, C.G., Sadd, P.A. (2004). Chloropropanols and their esters in cereal products. Czech Journal of Food Sciences, 22, 259 262. 73. Zelinkov , Z., Svejkovsk , B., Vel ek, J., Dole al, M. (2006). Fatty acid esters of 3-chloropropane-1,2-diol in edible oils. Food Additives and Contaminants, 23, 1290 1298.
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